Effect Of Calcination Temperature On The Morphology Of Plating Sludge

نویسندگان

  • N. Tugrul
  • O. Dere Ozdemir
  • S. Piskin
چکیده

Abstract— The effect of calcination temperature on the morphology of plating sludge generated from waste water treatment plant was studied. This waste was hazardous waste due to high toxic metal content [1]. It must be recovered, reuse or recycled before the process but its properties should determined in order to decide recovery method [2]. Previous researches were shown that this kind of wastes were used in different industries such as ceramic, glass, pigment, etc., at this point, its behavior against to heat was very important to decide the suitable recovery method [3,4,5]. In this study, the sludge was dried and calcined for 3 hours at temperatures ranging from 650 to 1200°C. Phase transformation of the calcined powders has been investigated as a function of calcination temperature by room-temperature X-ray diffraction and scanning electron microscopy techniques. With increasing calcining temperature, metal oxides were formed cubic spinel phase (ZnCr2O4) with calcium iron phosphate.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Effect of Calcination Temperature and Li / TFA Molar Ratio on Morphology and Phase of Lithium Fluoride Nanoparticles Produced by Fluorolytic Sol-Gel Method

In this research, synthesis of lithium fluoride (LiF) nanoparticles  by fluorolytic sol-gel method has been studied. Moreover, the effect of lithium ion to fluorine source molar ratio and calcination temperature on particle size and phase of LiF nanoparticles were investigated. Lithium acetate (C2H3LiO2), trifluoroacetic acid (TFA), ethylene glycol monobutyl ether and oleic acid were used as so...

متن کامل

Characterization of Cobalt Oxide Co3O4 Nanoparticles Prepared by Various Methods: Effect of Calcination Temperatures on Size, Dimension and Catalytic Decomposition of Hydrogen Peroxide

In this scientific research work we report a novel method to synthesis Co3O4 nanoparticles via calcinations of cobalt hydroxide which can be conveniently prepared by the Co(NO3 )2.6H2O with different reactants. In order to study the effect of calcination temperature on structure and morphology of the nanoparticles, the calcinations take place at various temperatures (at 300°C, 500°C and 700°C)....

متن کامل

From 4'-Hydroxy-2,2':6',2''-Terpyridine Complex of Chromium(III) towards Cr2O3 Nanoparticles: Effects of the Calcination Temperature on the Particle Size and Morphology

A new chromium(III) complex containing 4ʹ-hydroxy-2,2ʹ:6ʹ,2ʺ-terpyridine (tpyOH) has been prepared by the reaction of CrCl3. 6H2O with tpyOH in the presence of metallic zinc to afford the new complex [CrCl3(tpyOH)] (1). The complex 1 was used as a suitable precursor for the preparation of Cr2O3 nanoparticles by the simple calcination method at three different annealed temperatures of 400, 600, ...

متن کامل

تأثیر دما و زمان پخت بر خواص ساختاری و الکتریکی نانوذرات SrFeO

In this paper, nanoparticles of strontium hexaferrite (SrFe12O19) were synthesized via sol–gel technique. For preparation of the SrFe12O19 nanoparticles, the nitrates of the metal with a specified ratio of molar and citric acid were used. By using the thermogravimetric analysis (DTA/TGA) the final product was studied. On the basis of this analysis, the samples at different temperatures from 600...

متن کامل

The Use of Raw and Thermally-Modified Calcareous Sludge Generated in Stone Cutting Industry for Sulfur Dioxide Removal

Management of solid wastes is considered as an economic and environmental issue in the building stone industry. The current study uses raw and calcined calcareous sludge, generated in the stone cutting factories, in order to remove sulfur dioxide. Sludge characterization has been performed, using X-ray fluorescence (XRF), X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-d...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2010